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Mubychem Group, established in
1976, is the pioneer manufacturer of Zinc Chloride, Ammonium
Chloride, Calcium Chloride, Potassium Chloride, Sodium Acetate,
Sodium Thiosulphate, Pharmaceutical, Fragrance & Flavor chemicals in
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Calcium Chloride
for Technical Pure and IP Grade
Calcium Chloride USP
CaCl2·2H2O 147.01
Calcium chloride, dihydrate.
Assay— Calcium Chloride contains an amount of CaCl2 equivalent to not less than 99.0 percent and not more than 107.0 percent of CaCl2·2H2O.
Packaging and storage— Preserve in tight containers.
Labeling— Where Calcium Chloride is intended for use in hem dialysis, it is so labeled.
Identification— A solution (1 in 10) responds to the tests for Calcium and for Chloride
pH: between 4.5 and 9.2, in a solution (1 in 20).
Aluminum (where it is labeled as intended for use in hem dialysis)— the limit is 1 4g per g.
Iron, aluminum, and phosphate— To a solution (1 in 20) add 2 drops of 3 N hydrochloric acid and 1 drop of phenolphthalein TS. Then add ammonium chloride–ammonium hydroxide TS, drop wise, until the solution is faintly pink, add 2 drops in excess, and heat the liquid to boiling: no turbidity or precipitate is produced.
Heavy metals— the limit is 0.001%.
Limit of magnesium and alkali salts— Dissolve 1 g in about 50 mL of water, add 500 mg of ammonium chloride, and proceed as directed in the test for Limit of magnesium and alkali salts under Calcium Carbonate, beginning with “heat the solution, and boil for 1 minute”: the weight of the residue does not exceed 5 mg (1.0%).
Organic volatile impurities meets the requirements.
Calcium Chloride Dihydrate as per BP Specifications
Calcium chloride, dihydrate
CaCl2,2H2Oı
Preparations
Calcium Chloride Injection
Compound Sodium Lactate Intravenous Infusion
DEFINITION
Content
97.0 per cent to 103.0 per cent of CaCl2,2H2O.
CHARACTERS
Appearance
White or almost white, crystalline powder, hygroscopic.
Solubility
Freely soluble in water, soluble in ethanol (96 per cent).
IDENTIFICATION
ıA. Solution S (see Tests) gives reaction of chlorides.
ıB. It gives the reactions of calcium.
ıC. It complies with the limits of the assay.
TESTS
Solution S
Dissolve 10.0 g in carbon dioxide-free water prepared from distilled water and dilute to 100 ml with the same solvent.
Appearance of solution
Solution S is clear and not more intensely coloured than reference solution.
Acidity or alkalinity
To 10 ml of freshly prepared solution S add 0.1 ml of phenolphthalein solution. If the
solution is red, not more than 0.2 ml of 0.01 M hydrochloric acid is required to discharge the colour and if the solution is colourless, not more than 0.2 ml of 0.01 M sodium hydroxide is required to turn it red.
Sulphates
Maximum 300 ppm.
Aluminium
To 10 ml of solution S add 2 ml of ammonium chloride solution R and 1 ml of dilute ammonia and boil the solution. No turbidity or precipitate is formed.
If intended for use in the manufacture of dialysis solutions, the above test is replaced by the test for aluminium maximum 1 ppm.
Barium
To 10 ml of solution S add 1 ml of calcium sulphate solution R . After at least 15 min, any opalescence in the solution is not more intense than that in a mixture of 1 ml of distilled water and 10 ml of solution S.
Iron
Maximum 10 ppm, determined on solution S.
Magnesium and alkali metals
Maximum 0.5 per cent.
Heavy metals
Maximum 20 ppm.
Calcium Chloride Hexahydrate as per BP Specifications
Calcium chloride, hexahydrate
CaCl2,6H2O
DEFINITION
Content
97.0 per cent to 103.0 per cent of CaCl2,6H2O.
CHARACTERS
Appearance
White or almost white, crystalline mass or colourless crystals.
Solubility
Very soluble in water, freely soluble in ethanol (96 per cent).
It solidifies at about 29 °C.
IDENTIFICATION
ıA. Solution S (see Tests) gives reaction of chlorides.
ıB. It gives the reactions of calcium.
ıC. It complies with the limits of the assay.
TESTS
Solution S
Dissolve 15.0 g in carbon dioxide-free water prepared from distilled water R and dilute to 100 ml with the same solvent.
Appearance of solution
Solution S is clear and not more intensely coloured than reference solution.
Acidity or alkalinity
To 10 ml of freshly prepared solution S add 0.1 ml of phenolphthalein solution. If the solution is red, not more than 0.2 ml of 0.01 M hydrochloric acid is required to discharge the colour and if the solution is colourless, not more than 0.2 ml of 0.01 M sodium hydroxide is required to turn it red.
Sulphates
Maximum 200 ppm.
Aluminium
To 10 ml of solution S add 2 ml of ammonium chloride solution R and 1 ml of dilute ammonia R1 . Heat to boiling. No turbidity or precipitate is formed. If intended for use in the manufacture of dialysis solutions, the above test is replaced by the test for aluminium : maximum 1 ppm.
Barium
To 10 ml of solution S add 1 ml of calcium sulphate solution. After at least 15 min, any opalescence in the solution is not more intense than that in a mixture of 1 ml of distilled water and 10 ml of solution S.
Iron
Maximum 7 ppm, determined on solution S.
Magnesium and alkali metals
Maximum 0.3 per cent.
Heavy metals
Maximum 15 ppm.
Calcium Chloride Injection as per USP Specifications
Calcium Chloride Injection is a sterile solution of Calcium Chloride in Water for Injection. It contains not less than 95.0 percent and not more than 105.0 percent of the labeled amount of CaCl2·2H2O.
Packaging and storage— Preserve in single-dose containers, preferably of Type I glass.
Labeling— The label states the total osmolar concentration in mOsmol per L. Where the contents are less than 100 mL, or where the label states that the Injection is not for direct injection but is to be diluted before use, the label alternatively may state the total osmolar concentration in mOsmol per mL.
Identification— It responds to the tests for Calcium and Chloride.
Bacterial end toxins— It contains not more than 0.2 USP End toxin Unit per mg of calcium chloride.
pH: between 5.5 and 7.5 in the undiluted Injection, except where the concentration is greater than 1 in 20, in which case this range applies to the Injection diluted with water to yield a concentration of 1 in 20.
Particulate matter: meets the requirements for small-volume injections.
Other requirements— It meets the requirements under Injections 1.
Calcium Chloride as per US Food Chemical Codex
CaCl2 Formula wt, anhydrous 110.98
CaCl2·2H2O Formula wt, dihydrate 147.01
DESCRIPTION
Calcium Chloride occurs as white, hard fragments, granules, or powder. It is anhydrous or contains two molecules of water of hydration. It is deliquescent. It is soluble in water and
slightly soluble in alcohol. The pH of a 1:20 aqueous solution is between 4.5 and 11.0.
Function Firming agent.
REQUIREMENTS
Labeling Indicate whether it is anhydrous or the dihydrate.
Identification A 1:10 aqueous solution gives positive tests for Calcium and for Chloride,
Assay Anhydrous: Not less than 93.0% and not more than 100.5% of CaCl2; Dihydrate: Not less than 99.0% and not more than 107.0% of CaCl2·2H2O.
Acid-Insoluble Matter Anhydrous: Not more than 0.02%; no particles per kilogram of sample greater than 2 mm in any dimension.
Arsenic Not more than 3 mg/kg.
Fluoride Not more than 0.004%.
Lead Not more than 5 mg/kg.
Magnesium and Alkali Salts Anhydrous: Not more than 5.0%; Dihydrate: Not more than 4.0%.
Calcium Chloride Solution as per US Food Chemical Codex
DESCRIPTION
Calcium Chloride Solution occurs as a clear to slightly turbid, colorless or slightly colored liquid at room temperature. It is normally available in a concentration range of about 35% to 45% of CaCl2.
Function Sequestrant; firming agent.
REQUIREMENTS
Identification When diluted to a concentration of about 1:10 (CaCl2 basis), a sample gives positive tests for Calcium and for Chloride.
Assay Not less than 90.0% and not more than 110.0%, by weight, of the labeled amount of calcium chloride, expressed as CaCl2.
Alkalinity [as Ca(OH)2] Not more than 0.3%.
Fluoride Not more than 0.004%, calculated on the amount of CaCl2 as determined in the Assay.
Lead Not more than 4 mg/kg, calculated on the amount of CaCl2 as determined in the Assay.
Magnesium and Alkali Salts Not more than 5.0%, calculated on the amount of Calcium Chloride as determined in the Assay.
Calcium Chloride Dihydrate as per ACS specifications
CaCl2 .
2H2O
Formula Wt 147.01
CAS Number 10035-04-8
REQUIREMENTS
|
Assay |
99.0-105.0% CaCl2 . 2H2O |
|
pH of a 5% solution |
4.5-8.5 at 25 |
C
MAXIMUM ALLOWABLE
|
Insoluble matter |
0.01% |
|
Oxidizing substances (as NO3) |
0.003% |
|
Sulfate (SO4) |
0.01% |
|
Ammonium (NH4) |
0.005% |
|
Barium (Ba) |
0.005% |
|
Heavy metals (as Pb) |
5 ppm |
|
Iron (Fe) |
0.001% |
|
Magnesium (Mg) |
0.005% |
|
Potassium (K) |
0.01% |
|
Sodium (Na) |
0.02% |
|
Strontium (Sr) |
0.1% |
Calcium Chloride Desiccant
CaCl2
Formula Wt 110.98
CAS Number 10043-52-4
REQUIREMENTS
Assay 
96.0%
CaCl2
MAXIMUM ALLOWABLE
Titrable base 0.006 meq/g
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Calcium Chloride Manufacturer manufacturer:
MUBY CHEMICALS
S-8, SARIFA MANSION, 2ND FLANK ROAD, CHINCHBUNDER, MUMBAI
400009, INDIA.
TEL: (OFFICE) 91-22-23770100, 23726950, 23774610, 23723564.
FAX: 91-22-23728264.
e-mail: info@mubychem.com
Copyright
and Usual
Disclaimer
is Applicable.
Last
updated: 05 May, 2010.
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