Xanthan Gum BP Ph Eur IP EP USP NF FCC Food Grade Manufacturers, with SDS MSDS Sheet

Supplier, Manufacturer, Exporter of Xanthan Gum IP BP Ph Eur EP USP NF FCC Food Grade, Muby Chemicals of Mubychem Group, established in 1976, is the original manufacturers of Specialty Chemicals, Pharmaceutical Excipient, Fragrance Food & Flavor chemicals, Reagent Grade Chemicals, Shale Gas Fracturing Chemicals in India. Mubychem Group has several manufacturing facilities spread across Western India and world wide contacts and toll manufacturers. We are exporting globally to countries like USA, Canada, Europe, UAE, South Africa, Tanzania, Kenya, Egypt, Nigeria, Cameroon, Uganda, Turkey, Mexico, Brazil, Chile, Argentina, Dubai, Korea, Vietnam, Thailand, Malaysia, Indonesia, Australia, China, Germany, France, Italy, Portugal, Bangladesh, etc.

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Xanthan Gum: CAS Number: 11138-66-2, EINECS EC Number: 234-394-2, Molecular Formula: C35H49O29 (monomer), Molecular Weight: -, HS Code ---**

Specifications, Safety Data Sheet, Manufacturing process details, Wholesale retail buy sell prices, Uses etc available on line in these pages for Xanthan Gum.

Xanthan Gum BP Ph Eur Grade Specifications
Ph Eur
Action and use: Excipient.

DEFINITION
High-molecular-mass anionic polysaccharide produced by fermentation of carbohydrates with Xanthomonas campestris.
Xanthan gum has a relative molecular mass of approximately 1 × 106. It exists as the sodium, potassium or calcium salt.
Content: Minimum 1.5 per cent of pyruvoyl groups (C3H3O2; Mr 71.1) (dried substance).

CHARACTERS
Appearance: White or yellowish-white, free-flowing powder.
Solubility: Soluble in water giving a highly viscous solution, practically insoluble in organic solvents.
IDENTIFICATION
A. In a flask, suspend 1 g in 15 ml of 0.1 M hydrochloric acid . Close the flask with a fermentation bulb containing barium hydroxide solution and heat carefully for 5 min. The barium hydroxide solution shows a white turbidity.
B. To 300 ml of water, previously heated to 80 °C and stirred rapidly with a mechanical stirrer in a 400 ml beaker, add, at the point of maximum agitation, a dry blend of 1.5 g of carob bean gum and 1.5 g of the substance to be examined. Stir until the mixture forms a solution, and then continue stirring for 30 min or longer. Do not allow the water temperature to drop below 60C during stirring. Discontinue stirring and allow the mixture to stand for at least 2 h. A firm rubbery gel forms after the temperature drops below 40C but no such gel forms in a 1 per cent control solution of the sample prepared in the same manner but omitting the carob bean gum.

TESTS
pH: 6.0 to 8.0 for a 10.0 g/l solution.
Viscosity: Minimum 600 mPa·s.
2-Propanol: To pass Gas chromatography test. Limit 2-propanol: maximum 750 ppm.
Other polysaccharides: To pass Thin-layer chromatography test.
Loss on drying: Maximum 15.0 per cent, determined on 1.000 g by drying in an oven at 105 °C for 2.5 h.
Total ash: 6.5 per cent to 16.0 per cent.
Microbial contamination: Total viable aerobic count not more than 103 bacteria and 102 fungi per gram, determined by plate count. It complies with the test for Escherichia coli.

Xanthan Gum USP NF Grade Specifications
Xanthan Gum is a high molecular weight polysaccharide gum produced by a pure-culture fermentation of a carbohydrate with Xanthomonas campestris, then purified by recovery with Isopropyl Alcohol, dried, and milled. It contains Dglucose and D-mannose as the dominant hexose units, along with D-glucuronic acid, and is prepared as the sodium, potassium, or calcium salt. It yields not less than 4.2 percent and not more than 5.0 percent of carbon dioxide, calculated on the dried basis, corresponding to not less than 91.0 percent and not more than 108.0 percent of Xanthan Gum.

Identification: To 300 mL of water in a 400-mL beaker, previously heated to 80 and stirred rapidly by mechanical means, add, at the point of maximum agitation, a dry blend of 1.5 g of Xanthan Gum and 1.5 g of locust bean gum. Stir until the mixture dissolves, and then continue stirring for 30 minutes longer. Do not allow the temperature of the mixture to drop below 60 during the stirring. Discontinue stirring, and allow the mixture to cool at room temperature for not less than 2 hours: a firm, rubbery gel forms after the temperature drops below 40 , but no such gel forms in a control solution prepared in the same manner with 3.0 g of Xanthan Gum and without locust bean gum.
Viscosity: Place 250 mL of water in a 400-mL beaker, and add a dry blend of 3.0 g of Xanthan Gum and 3.0 g of potassium chloride slowly while stirring at 800 rpm, using a low-pitched propeller-type stirrer. Add an additional quantity of 44 mL of water, rinsing the walls of the beaker. Approximately 10 minutes after the addition of the dry blend of Xanthan Gum and the potassium chloride to the water, remove the beaker from the propeller-type stirrer, and vigorously stir the solution by hand to ensure that all the particles around the edge of the beaker are in solution. Return the beaker to the stirrer, and agitate at 800 rpm for a total mixing time of 2 hours. Then adjust the temperature to 24±1C, and stir by hand in a vertical motion to eliminate any thixotropic effects or layering.
[NOTE—Each hand mixing should be not more than 15 to 30 seconds, and the last hand mixing should occur immediately prior to measuring the viscosity.] Equip a suitable rotational viscosimeter with a spindle having a cylinder 1.27 cm in diameter and 0.16 cm high attached to a shaft 0.32 cm in diameter, the distance from the top of the cylinder to the lower tip of the shaft being 2.54 cm, and the immersion depth being 5.00 cm (No. 3 spindle). With the spindle rotating at 60 rpm, immediately observe and record the scale reading. Convert the scale readings to centipoise by multiplying the readings by the constant for the viscosimeter spindle and speed employed. The viscosity at 24 is not less than 600 centipoise.
Microbial limits: It meets the requirements of the tests for Salmonella species and Escherichia coli.
Loss on drying: Dry it at 105 for 2.5 hours: it loses not more than 15.0% of its weight.
Ash: Accurately weigh about 3 g in a tared crucible, and incinerate at about 650 until free from carbon. Cool the crucible and its contents in a desiccator, and weigh: the weight of the ash is between 6.5% and 16.0%, calculated on the dried basis.
Arsenic: 3 ug per g.
Lead: the limit is 5 @g per g.
Heavy metals: The limit is 0.003%.
Limit of isopropyl alcohol: To pass the test, not more than 0.075% is found.
Pyruvic acid: To pass the test.

DESCRIPTION
Xanthan Gum occurs as a cream colored powder. It is a high-molecular-weight polysaccharide gum produced by a pureculture fermentation of a carbohydrate with Xanthomonas campestris, purified by recovery with isopropyl alcohol, dried, and milled. It contains D-glucose and D-mannose as the dominant hexose units, along with D-glucuronic acid and pyruvic acid, and it is prepared as the sodium, potassium, or calcium salt. It is readily soluble in hot or cold water, but it is insoluble in alcohol. Its solutions are neutral.
Function: Stabilizer; thickener; emulsifier; suspending agent; bodying agent; foam enhancer.

REQUIREMENTS
Identification: Transfer 300 mL of water, previously heated to 80°, into a 400-mL beaker and stir rapidly with a mechanical stirrer. At the point of maximum agitation, add a dry blend of 1.5 g of sample and 1.5 g of locust bean gum. Stir until the mixture goes into solution, and then continue stirring for 30 min longer. Do not allow the water temperature to drop below 60°. Discontinue stirring, and allow the mixture to cool at room temperature for at least 2 h. A firm, rubbery gel forms after the temperature of the mixture drops below 40°. No such gel forms in a 1% control solution of sample prepared in the same manner but omitting the locust bean gum.
Assay: A sample yields, on the dried basis, not less than 4.2% and not more than 5.4% of carbon dioxide (CO2), corresponding to between 91.0% and 117.0% of Xanthan Gum.
Isopropyl Alcohol: Not more than 0.075%.
Lead: Not more than 2 mg/kg.
Loss on Drying: Not more than 15.0%.
Pyruvic Acid: Not less than 1.5%.
Viscosity: Passes test.

For Original Monographs of IP Indian Pharmacopoeia BP British Pharmacopoeia USP US Pharmacopoeia FCC Food Grade product, please check with the respective web-pages or books.

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Xanthan Gum SDS, Safety Data Sheet
MSDS Sheet, Material Safety Data Sheet 23-Nov-20

Product Name & Other Names: Xanthan Gum, Polysaccharide gum produced by the fermentation of carbohydrate with the bacterium Xanthomonas campestris.
CAS Number: 11138-66-2
EINECS EC Number: 234-394-2
Molecular Weight: -
Molecular Formula: (C35H49O29)n
Relevant uses and uses advised against (if any): Industrial Manufacturing.
Suppliers: As per letterhead.

GHS, Globally Harmonized System Classification in accordance with 29 CFR 1910
Classification according to Regulation (EC) No 1272/2008

Not a hazardous substance or mixture according to Regulation (EC) No. 1272/2008.
This substance is not classified as dangerous according to Directive 67/548/EEC.

Hazards not otherwise classified (HNOC):
May causes mild skin irritation.
May causes mild eye irritation.

Precautionary statements:
P261: Avoid breathing dust/fume/gas/mist/vapors/spray.
P262: Do not get in eyes, on skin, or on clothing.
P281: Use personal protective equipment as required.
P302+P352 - IF ON SKIN: Wash with plenty of soap and water.
P303+P361+P353 - IF ON SKIN (or hair): Remove/Take off immediately all contaminated clothing. Rinse skin with water/shower.
P304+P340: IF INHALED: Remove victim to fresh air and keep at rest in a position comfortable for breathing.
P305+P351+P338: IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing.
P337+313: If eye irritation persists get medical advice/attention.

Always get medical attention after the first aid is over.
Emergency and First Aid Procedures:
Eyes - Flush with water for at least 15 minutes, raising and lowering eyelids occasionally. Get medical attention if irritation persists.
Skin - Thoroughly wash exposed area for at least 15 minutes. Remove contaminated clothing. Launder contaminated clothing before reuse. Get medical attention if irritation persists.
Ingestion - If Xanthan Gum is swallowed, if conscious, give plenty of water. Immediately call a physician. Never give anything by mouth to an unconscious person.
Inhalation - Remove to fresh air. Give oxygen if breathing is difficult; give artificial respiration if breathing has stopped. Get medical attention.

Extinguisher Media: Use media suitable to extinguish surrounding fire. Use water spray, alcohol-resistant foam, dry chemical, or carbon dioxide. Do not use a solid water stream as it may scatter and spread fire.
Auto-ignition Temperature: > 200 deg C (> 392.00 deg F)
Flammable Limits in Air % by Volume: N/A. This material in sufficient quantity and reduced particle size can create a dust explosion.
Special Information: In the event of a fire, wear full protective clothing and NIOSH-approved self-contained breathing apparatus with full face piece operated in the pressure demand or other positive pressure mode. At high temperatures under fire conditions, it may produce toxic or irritating fumes. Fire-extinguishing work is done from the windward and the suitable fire-extinguishing method according to the surrounding situation is used. Uninvolved persons should evacuate to a safe place.

Personal precautions, protective equipment, and emergency procedures: Avoid generating dusty conditions. Avoid breathing dust/fumes/gas/mist/vapors/spray. Use individual protective equipment (waterproof boots, suitable protective clothing, safety glasses, etc.). Restrict unprotected personnel from the area. Prevent any contact with hot surfaces. Do not approach facing the wind. Do not touch the spilled material.
Environmental precautions: Do not let the product enter drains, soil, or water sources.
Methods and materials used for containment Cleanup procedures and Storage: Contain spilled material. Cover with an inert, non-combustible absorbent material, (e.g. sand, earth, diatomaceous earth, vermiculite). Vacuum or sweep-up and remove to an approved disposal container.

Precautions for safe handling: Apply according to good manufacturing and industrial hygiene practices. Ensure proper ventilation. Wash thoroughly after handling. Do not drink, eat, or smoke while handling. Avoid contact with skin, eyes, and clothing. Minimize dust generation. Avoid breathing dust/fumes/gas/mist/vapors/spray. Avoid contact with eyes, skin, and clothing. Keep container tightly closed. Avoid ingestion and inhalation. Use individual protective equipment (waterproof boots, suitable protective clothing, safety glasses, etc.). Prevent any contact with hot surfaces.
Conditions for safe storage, including any incompatibilities: Store in cool, dry, and ventilated area away from heat sources and protected from sunlight in tightly closed original container. Keep air contact to a minimum. Do not leave the material container open. Store protected from heat, sparks and ignition sources and incompatible materials. Avoid contact with skin and eyes. Avoid inhalation of dust/mist/vapor. Do not store with incompatible materials like strong oxidizing and reducing agents, strong acids, and bases.

This product is not known to contain any hazardous materials with occupational exposure limits established by the region-specific regulatory bodies. As an airborne dust, exposure limits pertaining to "particulates not otherwise regulated" have been provided below.
ACGIH TLV: TWA: 10 mg/m3 inhalable particles, recommended; TWA: 3 mg/m3 respirable particles, recommended
OSHA PEL: TWA: 15 mg/m3 total dust; TWA: 5 mg/m3 respirable fraction
Ventilation System: A system of local and/or general exhaust is recommended to keep employee exposures as low as possible. Local exhaust ventilation is generally preferred because it can control the emissions of the contaminant at its source, preventing dispersion of it into the general work area.
Personal Respirators (NIOSH Approved): For conditions of use where exposure to dust or mist is apparent and engineering controls are not feasible, a particulate respirator may be worn. For emergencies or instances where the exposure levels are not known, use a full-face positive-pressure, air-supplied respirator.
Skin Protection: Wear protective gloves and clean body-covering clothing.
Eye Protection: Use chemical safety goggles and/or full face shield where dusting or splashing of solutions is possible. Maintain eye wash fountain and quick-drench facilities in work area.
Other Control Measures: Maintain good housekeeping in work area. Dust deposits on floors and other surfaces may pick up moisture and cause the surfaces to become slippery and present safety hazards. Handle in accordance with good industrial hygiene and safety practice. Wash hands after handling.

Appearance and Odor: Cream to Light yellow Solid material with Characteristic odor.
pH: Neutral
Odor: Characteristic odor.
Odor threshold: Not available.
pH: Not available.
Relative density: 0,7 to 0,8
Melting point/freezing point: Not available.
Boiling Point: Decomposes
Flash point: Not available.
Auto ignition Temperature: >200C
Decomposition temperature: Not available.
Upper/lower flammability or explosive limits: Not available.
Vapor pressure: Not available.
Vapor density: Not available.
Evaporation rate: Not available.
Flammability (solid, gas): Not available.
Partition coefficient: n-octanol/water: Not available.
Solubility in Water: Soluble.
Viscosity: Not available.
Molecular Weight: -
Molecular Formula: (C35H49O29)n

10. REACTIVITY DATA

Stability: Stable
Conditions to Avoid: Heat, humidity, Dust generation.
Incompatibility (Materials to Avoid): Strong oxidizing and reducing agents, Strong acids and bases.
Hazardous Decomposition Products: Carbon monoxide, carbon dioxide
Hazardous Polymerization: Will not occur.

Toxicity Data:
LC50 Inhalation Dusts and mists Rat 21 mg/l 1 hours
LD50 Oral Mouse 20000 mg/kg -
LD50 Oral Rat 45000 mg/kg -
Carcinogenicity: This product present at levels greater than or equal to 0.1% is identified as probable, possible or confirmed human carcinogen by IARC, NTP, ACGIH & OSHA.
Mutagenicity: No known significant effects or critical hazards.
Teratogenicity: No known significant effects or critical hazards.
Developmental effects: No known significant effects or critical hazards.
Fertility effects: No known significant effects or critical hazards.

Toxicity to fish: LC50 - Oncorhynchus mykiss (rainbow trout) - 320 - 560 mg/l - 96 h
Toxicity: Avoid release into the environment. Runoff from fire control or dilution water may cause pollution.
Bioaccumulative potential: Does not bioaccumulate.
Mobility: Likely to be mobile due to water solubility.
Results of PBT and vPvB assessment: No data available for assessment.

Waste Disposal Methods: Dispose Xanthan Gum in accordance with all applicable Federal, State and Local regulations.

DOT USA, TDG Canada & ADR/RID Europe: Not regulated.
IMDG/IMO: Not regulated.
IATA/ICAO: Not regulated.

USA Regulations:
SARA Section 302 Extremely Hazardous Substances: None of the chemicals in this product have a TPQ.
Section 313: No chemicals are reportable under Section 313.
California Proposition 65: This product is not known to contain chemicals listed under Proposition 65.

Disclaimer:
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Our company provides this MSDS sheet in good faith but makes no representation as to its comprehensiveness or accuracy. This SDS sheet is intended only as a guide to the appropriate precautionary handling of the material by a properly trained person using this product. The above information has been compiled from various sources and has the possibility of discrepancy and being out-dated information. Individuals receiving the information must exercise their independent judgment and do further search in determining its appropriateness for a particular purpose. In no case shall our company be liable to loss or damages by the product user.
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