Vanillin or 4-Hydroxy-3-methoxybenzaldehyde, Vanillic aldehyde Manufacturers, with SDS GHS MSDS Sheet |
Supplier, Manufacturer, Exporter of Vanillin, Muby Chemicals of Mubychem Group, established in 1976, is the original manufacturers of Specialty Chemicals, Pharmaceutical Excipient, Fragrance Food & Flavor chemicals, Reagent Grade Chemicals, Shale Gas Fracturing Chemicals in India. Mubychem Group has several manufacturing facilities spread across Western India and world wide contacts and toll manufacturers. We are exporting globally to countries like USA, Canada, Europe, UAE, South Africa, Tanzania, Kenya, Egypt, Nigeria, Cameroon, Uganda, Turkey, Mexico, Brazil, Chile, Argentina, Dubai, Korea, Vietnam, Thailand, Malaysia, Indonesia, Australia, China, Germany, France, Italy, Portugal, Bangladesh, etc. The products are offered as per required specifications and in correct shape and size in mm or meshs or microns as specified by the buyer. The participating units have one or more accreditations like FDA - cGMP and GLP approval, ISO-9001 Certified, "REACH" Registered, ISO-14001, ISO/IEC 17025, ISO-22000, FSSC 22000, ISO 45001, Kosher Certified, Halal Certified, HACCP, FSSAI. We offer Commercial Pure & IP BP EP Ph Eur USP NF JP FCC Food Grade Analytical Reagent Grades of Chemicals |
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Vanillin or 4-Hydroxy-3-methoxybenzaldehyde, Vanillic aldehyde: CAS Number: 121-33-5, EINECS EC Number: 204-465-2, Molecular Formula: 4-(HO)C6H3-3-(OCH3)CHO or C8H8O3, Molecular Weight: 152.15, FEMA Number: 3107, HS Code ---**
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SDS MSDS Sheet of Vanillin or 4-Hydroxy-3-methoxybenzaldehyde, Vanillic aldehyde Manufacturers
Vanillin
4-Hydroxy-3-methoxybenzaldehyde, Vanillic aldehyde Pure Suppliers
Vanillin is the primary chemical component of the extract of the vanilla bean. Synthetic vanillin is an aromatic compound, Vanillin, as its name implies, is the major flavor component of vanilla. It is mostly used in foods, beverages, perfumes and pharmaceuticals.
Vanillin and ethylvanillin are used by the food industry; ethylvanillin is more expensive but has a stronger note. It differs from vanillin by having an ethoxy group (−O−CH2CH3) instead of a methoxy group (−O−CH3). Vanillin can be used as a general-purpose stain for visualizing spots on thin-layer chromatography plates.
General Properties and Specifications of Vanillin:
Appearance: White to off-white powder or crystals.
Odor: Sweet characteristic.
Assay: 99% minimum.
Melting point: 81C to 83C.
Boiling point: 170C literature.
Specifications of Vanillin USP NF Grade:
C8H8O3 152.15
Benzaldehyde, 4-hydroxy-3-methoxy-.
Vanillin --- CAS 121-33-5.
Vanillin contains not less than 97.0 percent and not more than 103.0 percent of C8H8O3, calculated on the dried basis.
Packaging and storage: Preserve in tight, light-resistant containers.
Identification:
A: Infrared Absorption.
B: Ultraviolet Absorption
Melting range: between 81 and 83 .
Loss on drying: Dry it over silica gel for 4 hours: it loses not more than 1.0% of its weight.
Residue on ignition: not more than 0.05%.
Assay: Transfer about 100 mg of Vanillin, accurately weighed, to a 250-mL volumetric flask, add methanol to volume, and mix. Pipet 2 mL of this solution into a 100-mL volumetric flask, add methanol to volume, and mix. Dissolve an accurately weighed quantity of USP Vanillin RS in methanol and dilute quantitatively and stepwise with methanol to obtain a Standard solution having a known concentration of about 8 microg per mL. Concomitantly determine the absorbances of both solutions in 1-cm cells at the wavelength of maximum absorbance at about 308 nm, with a suitable spectrophotometer, using methanol as the blank. Calculate the quantity, in mg, of C8H8O3 in the portion of Vanillin taken by the formula:
12.5C( AU / AS )
in which C is the concentration, in microg per mL, of USP Vanillin RS in the Standard solution; and AU and AS are the absorbances of the solution of Vanillin and the Standard solution, respectively.
Specifications of Vanillin BP Ph Eur Grade:
C8H8O3 --- 152.1 --- CAS 121-33-5
DEFINITION
Vanillin contains not less than 99.0 per cent and not more than the equivalent of 101.0 per cent of 4-hydroxy-3-methoxybenzaldehyde, calculated with reference to the dried substance.
CHARACTERS
White or slightly yellowish, crystalline powder or needles, slightly soluble in water, freely soluble in alcohol and in methanol. It dissolves in dilute solutions of alkali hydroxides.
IDENTIFICATION
First identification: B
Second identification: A, C, D
A. Melting point: 81C to 84C.
B. Examine by infrared absorption spectrophotometry, comparing with the spectrum obtained with vanillin CRS. Examine the substances prepared as discs.
C. Examine the chromatograms obtained in the test for related substances in daylight after spraying. The principal spot in the chromatogram obtained with test solution (b) is similar in position, colour and size to the principal spot in the chromatogram obtained with reference solution (a).
D. To 5 mL of a saturated solution of the substance to be examined add 0.2 mL of ferric chloride solution. A blue colour is produced. Heat to 80C. The solution becomes brown. On cooling, a white precipitate is formed.
TESTS
Appearance of solution: Dissolve 1.0 g in alcohol and dilute to 20 mL with the same solvent. The solution is clear and not more intensely coloured than reference solution B.
Related substances: To pass the chromatographic test.
Any spot in the chromatogram obtained with test solution (a), apart from the principal spot, is not more intense than the spot in the chromatogram obtained with reference solution (b) (0.5 per cent).
Reaction with sulfuric acid: Dissolve 50 mg in 5 mL of sulfuric acid. After 5 min, the solution is not more intensely coloured than a mixture of 4.9 mL of yellow primary solution and 0.1 mL of red primary solution or a mixture of 4.9 mL of yellow primary solution and 0.1 mL of blue primary solution.
Loss on drying: Not more than 1.0 per cent, determined on 1.000 g by drying in a desiccator for 4 h.
Sulfated ash: Not more than 0.05 per cent, determined on 2.0 g.
ASSAY
Dissolve 0.120 g in 20 mL of alcohol and add 60 mL of carbon dioxide-free water. Titrate with 0.1 M sodium hydroxide, determining the end-point potentiometrically.
1 mL of 0.1 M sodium hydroxide is equivalent to 15.21 mg of C8H8O3.
Store protected from light.
For Original Monographs of IP Indian Pharmacopoeia BP British Pharmacopoeia USP US Pharmacopoeia FCC Food Grade product, please check with the respective web-pages or books.
Manufacturers:
MUBY CHEMICALS
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Vanillin or 4-Hydroxy-3-methoxybenzaldehyde, Vanillic aldehyde SDS GHS, MSDS Sheet, Material Safety Data Sheet
MSDS Sheet, Material Safety Data Sheet 23-Nov-20
Section 1: Chemical Product and Company Identification
Product Name & Other Names: Vanillin or 4-Hydroxy-3-methoxybenzaldehyde, Vanillic aldehyde.
CAS Number: 121-33-5
EINECS EC Code: 204-465-2
FEMA Number: 3107
Molecular Formula: 4-(HO)C6H3-3-(OCH3)CHO or C8H8O3
Molecular Weight: 152.15
Relevant uses and uses advised against (if any): Industrial Manufacturing.
Suppliers: As per letterhead.
Section 2: Hazards Identification
GHS, Globally Harmonized System Classification in accordance with 29 CFR 1910
Hazard Class and Category Code(s), Regulation (EC) No 1272/2008 (CLP)
Not a hazardous substance or mixture according to Regulation (EC) No. 1272/2008.
This substance is not classified as dangerous according to Directive 67/548/EEC.
Labeling Regulation as per GHS & EC 1272/2008 (CLP) & GHS
GHS Label Elements NONE |
Signal Word: None
Hazards not otherwise classified (HNOC):
May causes mild skin irritation.
May causes mild eye irritation.
Precautionary statements:
P261: Avoid breathing dust/fume/gas/mist/vapors/spray.
P262: Do not get in eyes, on skin, or on clothing.
P281: Use personal protective equipment as required.
P302+P352: IF ON SKIN: Wash with plenty of soap and water.
P303+P361+P353: IF ON SKIN (or hair): Remove/Take off immediately all contaminated clothing. Rinse skin with water/shower.
P304+P340: IF INHALED: Remove victim to fresh air and keep at rest in a position comfortable for breathing.
P305+P351+P338: IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing.
P337+313: If eye irritation persists get medical advice/attention.
Section 3: Composition and Information on Ingredients
Product Name & Other Names: Vanillin or 4-Hydroxy-3-methoxybenzaldehyde, Vanillic aldehyde.
CAS Number: 121-33-5
EINECS EC Code: 204-465-2
FEMA Number: 3107
Section 4: First Aid Measures
Always seek medical advice after the first aid treatment.
Skin: Rinse with water. Soap may be used. Seek Medical Aid.
Eyes: Wash eyes with plenty of water for at least 15 minutes, lifting lids occasionally. Seek Medical Aid.
Inhalation: Remove to fresh air. If not breathing, give artificial respiration. If breathing is difficult, give oxygen.
Ingestion: If swallowed, induce vomiting immediately after giving two glasses of water. Never give anything by mouth to an unconscious person.
Section 5: Fire and Explosion Data
Flammability of the Product: Non-flammable.
Products of Combustion: Fumes and oxides of Carbon.
Fire Fighting Media and Instructions: Use water spray, alcohol-resistant foam, dry chemical or carbon dioxide. Wear self-contained breathing apparatus for firefighting if necessary.
Special Information: In the event of a fire, wear full protective clothing and NIOSH-approved self-contained breathing apparatus with full face piece operated in the pressure demand or other positive pressure mode. At high temperatures under fire conditions, it may produce toxic or irritating fumes. Fire-extinguishing work is done from the windward and the suitable fire-extinguishing method according to the surrounding situation is used. Uninvolved persons should evacuate to a safe place.
Section 6: Accidental Release Measures
Personal precautions, protective equipment and emergency procedures: Avoid breathing dust/fumes/gas/mist/vapors/spray. Ensure adequate ventilation. Use individual protective equipment (waterproof boots, suitable protective clothing, safety glasses, etc.). Restrict unprotected personnel from the area. Prevent any contact with hot surfaces. Do not approach facing the wind. Do not touch the spilled material.
Environmental precautions: Do not let the product enter drains, soil or water sources.
Methods and materials used for containment Cleanup procedures and Storage:
Small Spill: Use appropriate tools to put the spilled solid in a convenient waste disposal container. Finish cleaning by spreading water on the contaminated surface and dispose of according to legal requirements.
Large Spill: Contain spilled material. Do not inhale vapors, mist, or gas. Avoid dust formation. Use a shovel to put the material into a convenient waste disposal container. Finish cleaning by spreading water on the contaminated surface and allow to evacuate as per law.
Section 7: Handling and Storage
Precautions for safe handling: Apply according to good manufacturing and industrial hygiene practices. Ensure proper ventilation. Wash thoroughly after handling. Do not drink, eat or smoke while handling. Avoid contact with skin, eyes and clothing. Minimize dust generation. Avoid breathing dust/fumes/gas/mist/vapors/spray. Avoid contact with eyes, skin, and clothing. Keep container tightly closed. Avoid ingestion and inhalation. Use individual protective equipment (waterproof boots, suitable protective clothing, safety glasses, etc.). Prevent any contact with hot surfaces.
Conditions for safe storage, including any incompatibilities: Store in cool, dry and ventilated area away from heat sources and protected from sunlight in tightly closed original container. Keep air contact to a minimum. Do not leave the material container open. Store protected from heat, sparks and ignition sources and incompatible materials. Avoid contact with skin and eyes. Avoid inhalation of dust/mist/vapor. Do not store with incompatible materials like oxidizing agents. Air, light, and moisture sensitive.
Section 8: Exposure Controls/Personal Protection
Exposure Guidelines: This product does not contain any hazardous materials with occupational exposure limits established by the region-specific regulatory bodies.
Engineering Controls: Use process enclosures, local exhaust ventilation, or other engineering controls to keep airborne levels below recommended exposure limits. If user operations generate dust, fume or mist, use ventilation to keep exposure to airborne contaminants below the exposure limit.
Ventilation System: A system of local and/or general exhaust is recommended to keep employee exposures as low as possible. Local exhaust ventilation is generally preferred because it can control the emissions of the contaminant at its source, preventing dispersion of it into the general work area.
Personal Respirators (NIOSH Approved): For conditions of use where exposure to dust or mist is apparent and engineering controls are not feasible, a particulate respirator may be worn. For emergencies or instances where the exposure levels are not known, use a full-face positive-pressure, air-supplied respirator.
Skin Protection: Wear protective gloves and clean body-covering clothing.
Eye Protection: Use chemical safety goggles and/or full face shield where dusting or splashing of solutions is possible. Maintain eye wash fountain and quick-drench facilities in work area.
Other Control Measures: Maintain good housekeeping in work area. Dust deposits on floors and other surfaces may pick up moisture and cause the surfaces to become slippery and present safety hazards. Handle in accordance with good industrial hygiene and safety practice. Wash hands after handling.
Section 9: Physical and Chemical Properties
Physical state and appearance: White to off-white powder or crystals.
Odor: Sweet characteristic.
Odor threshold: Not available.
pH: Not available.
Relative density: Not available.
Melting point/freezing point: 81C to 83C
Initial boiling point and boiling range: 170C literature.
Flash point: Not available.
Auto-ignition temperature: Not available.
Decomposition temperature: Not available.
Upper/lower flammability or explosive limits: Not available.
Vapor pressure: Not available.
Vapor density: Not available.
Evaporation rate: Not available.
Flammability (solid, gas): Not available.
Partition coefficient: n-octanol/water: Not available.
Solubility: Slightly soluble in water, freely soluble in alcohol and in methanol. It dissolves in dilute solutions of alkali hydroxides.
Viscosity: Not available.
Molecular Formula: 4-(HO)C6H3-3-(OCH3)CHO or C8H8O3
Molecular Weight: 152.15
Section 10: Stability and Reactivity Data
Stability: It is stable in room temperature in closed containers under normal storage & handling.
Conditions of instability: Incompatible materials, Moisture
Incompatibility with various substances: Avoid high temperatures, sparks, open flames, light and moisture. Avoid contact with strong oxidizing agents.
Polymerization: Will not occur.
Section 11: Toxicological Information
LD50 Oral - Rat: > 1580 mg/kg
LD50 Dermal – Rat: > 5000 mg/kg
Carcinogenic Effects: Not a reported carcinogen by IARC, NTP, ACGIH, OSHA.
Reproductive toxicity: No data available.
Teratogenicity: No data available.
Developmental Effects: No data available.
The toxicological properties have not been fully investigated.
Section 12: Ecological Information
Toxicity to fish: flow-through test LC50 - Pimephales promelas (fathead minnow) - 57 mg/l - 96 h.
Toxicity to daphnia and other aquatic invertebrates: static test EC50 - Daphnia magna (Water flea) - 36,6 mg/l - 48 h
BOD5 and COD: Not available.
Mobility: Will likely be mobile in the environment due to its water solubility.
Persistence and Degradability: Unlikely to persist.
Bioaccumulation/ Accumulation: No information available. However unlikely to accumulate.
Section 13: Disposal Considerations
Waste Disposal: Waste must be disposed of in accordance with federal, state and local environmental control regulations.
Section 14: Transport Information
DOT (USA) & ADR/RID: Not dangerous goods.
IMDG/IMO: Not dangerous goods.
IATA/ICAO: Not dangerous goods.
Section 15: Other Regulatory Information
USA Regulations:
SARA 313: Not applicable.
SARA 311/312 Hazard Categories: Not applicable.
California Prop 65: California No Significant Risk Level: None of the chemicals in this product are listed.
Disclaimer:
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Our company provides this MSDS sheet in good faith but makes no representation as to its comprehensiveness or accuracy. This SDS sheet is intended only as a guide to the appropriate precautionary handling of the material by a properly trained person using this product. The above information has been compiled from various sources and has the possibility of discrepancy and being out-dated information. Individuals receiving the information must exercise their independent judgment and do further search in determining its appropriateness for a particular purpose. In no case shall our company be liable to loss or damages by the product user.
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